US EPA Method 537: Determination of Selected Perfluorinated Alkyl Acids in Drinking Water Using the Triple Quadrupole LCMS-8060

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EPA Method 537 is a solid phase extraction (SPE), liquid chromatography/tandem mass spectrometry (LC-MS/MS) method for selected perfluorinated compounds (PFCs) in drinking water.

This paper presents an evaluation of the instrumental portion of US EPA Method 537. It presents calibration ranges and estimated detection limits well below method requirements. In addition, the chromatography was shortened from the 25 minutes in EPA 537 to less than 10 minutes without loss of resolution.

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