Analysis times for semivolatile compounds can limit sample throughput and decrease overall lab productivity. You can significantly speed up methods on your existing GC-MS by using a properly scaled-down column and appropriately adjusted instrument conditions. The challenge with this approach is that the new conditions can result in oven ramp rates that exceed the performance of standard GC ovens, especially 120 V ovens. However, by using a GC Accelerator oven insert kit, Agilent 6890 and 7890 GCs can meet aggressive scaled-down oven programs, producing the same chromatographic separations in much less time.
In this technical article, an example of scaling down EPA Method 8270 and using a GC Accelerator kit to reduce cycle time is presented. Significantly faster semivolatiles analysis times were achieved, providing an opportunity for labs to increase sample throughput or process more rush samples.
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